NISHIYABU Kazuaki

    Department of Mechanical Engineering Professor
Last Updated :2024/04/25

Researcher Information

Degree

  • Docter of Engineering(Osaka University)

J-Global ID

Research Interests

  • マイクロ構造体   ナノインプリント   粉末成形   粉末射出成形   ナノ粉末   犠牲樹脂型   転写性   マイクロMIM   銅   ニッケル   焼結   コンタクト印刷   ナノ粒子   ナノファイバ   金属粉末射出成形   MIM   ポーラス材料   マイクロ加工   繊維強化複合材料   Porous Metals   Metal Injection Molding   Composite Materials   

Research Areas

  • Manufacturing technology (mechanical, electrical/electronic, chemical engineering) / Machine materials and mechanics
  • Nanotechnology/Materials / Material fabrication and microstructure control
  • Nanotechnology/Materials / Composite materials and interfaces
  • Manufacturing technology (mechanical, electrical/electronic, chemical engineering) / Manufacturing and production engineering
  • Nanotechnology/Materials / Nano/micro-systems
  • Nanotechnology/Materials / Nanomaterials

Academic & Professional Experience

  • 2016/04 - Today  Kindai UiniversityFaculty of Science and TechnologyProfessor
  • 2010/04 - 2016/03  Kinki UniversityFaculty of Science and EngineeringAssociate Professor
  • 2005/04 - 2010/03  Osaka Prefectural College of TechnologyIndustrial Systems EngineeringAssociate Professor
  • 1998/04 - 2005/03  Osaka Prefectural College of Technology Industrial Systems EngineeringDepartment of Mechanical EngineeringAssociate Professor
  • 1999/04 - 1999/09  Katholieke Universiteit LeuveDepartment of Metals and MaterialsGuest Professor
  • 1991/04 - 1998/03  Osaka Prefectural College of TechnologyDepartment of Mechanical EngineeringLecturer
  • 1992/04 - 1993/03  Osaka Prefectural Industrial Technical Research InstituteDivision of Material TechnologyReseacher
  • 1988/04 - 1991/03  Osaka Prefectural College of TechnologyDepartment of Mechanical EngineeringResearch Associate

Education

  • 1997/04 - 1999/03  Osaka University  Graduate School of Engineering  Division of Materials and Manufacturing Science
  • 1986/04 - 1988/03  Kinki University  Graduate School of Science and Engineering Research  Mechanical Engineering Course
  • 1982/04 - 1986/03  Kinki University  Faculty of Science and Engineering  Department of Mechanical Engineering

Association Memberships

  • The JAPAN SOCIETY FOR DIE AND MOLD TECHNOLOGY   THE JAPAN SOCIETY FOR TECHNOLOGY OF PLASTICITY   The Society for the Advancement of Material and Process Engineering   JAPAN SOCIETY OF COMPOSITES MATERIALS   THE SOCIETY OF MATERIAL SCIENCE, JAPAN   THE JAPAN SOCIETY OF MECHANICAL ENGINEERS   

Published Papers

  • TANABE Daiki; HORIUCHI Tokiyuki; NISHIMURA Souma; NISHIYABU Kazuaki
    Journal of the Society of Materials Science, Japan The Society of Materials Science, Japan 71 (6) 495 - 500 0514-5163 2021/10 [Refereed]
     
    This study aims to reveal the ultrasonic spot welding behavior and joining strength of carbon fiber reinforced thermoplastics (CFRTP) using carbon fiber reinforced energy director. The materials used for spot welding are woven carbon fiber reinforced poly phenylene sulfide (woven-CF/PPS) laminates and energy director consisting of spread carbon fiber and PPS polymer. The ultrasonic oscillator for the ultrasonic spot welding process has an oscillation frequency of 40 kHz and a maximum output of 600 W. The welding load and push-in amount of ultrasonic horn during welding process were precisely controlled by using an electric servo press machine. The effects of welding load and carbon fiber volume fraction in energy director on ultrasonic welding behavior and actual tensile shear strength were investigated to reveal the welding behaviour. The welding load and push-in amount of the ultrasonic horn was measured by a data logger. The welding part was evaluated by image analysis and cross-sectional observation using microscope. From the experimental results, it was revealed that the carbon fiber volume fraction in the energy director was significantly affects the ultrasonic welding behavior. According to the results of single lap tensile shear test, it was found that the actual tensile shear strength was increased by the addition of spread carbon fiber.
  • TANABE Daiki; HORIUCHI Tokiyuki; NISHIYABU Kazuaki
    Journal of the Society of Materials Science, Japan The Society of Materials Science, Japan 69 (5) 373 - 378 0514-5163 2020/05 [Refereed]
     
    This study aims to reveal the ultrasonic spot welding behavior of carbon fiber reinforced thermoplastics (CFRTP) using polymer based energy director. The materials used for spot welding are woven-CF/PPS laminates and energy director consisting of PPS polymer. The ultrasonic oscillator for the ultrasonic spot welding process has an oscillation frequency of 40 kHz and a maximum output of 600 W. The welding load and displacement of ultrasonic horn during welding process were precisely controlled by using an electric servo press machine. The effects of welding load and thickness of energy director on ultrasonic welding behavior and joining strength were investigated to reveal the welding behaviour. The temperature of the joining part during ultrasonic welding was measured by a ultrafine thermocouples, and the welding load and displacement of the horn was measured by the servo press machine. The welding part was evaluated by microscopic observation and cross-sectional observation using microscope and SEM. From the experimental results, it was revealed that the thickness of the energy director was significantly affects the ultrasonic welding behavior. From the result of single lap tensile shear test, it was found that the there was proper thickness of energy director to increase the joining strength.
  • TANABE Daiki; KUBOHORI Fumio; TAMURA Kouta; NISHIYABU Kazuaki
    Journal of the Society of Materials Science, Japan The Society of Materials Science, Japan 68 (2) 162 - 169 0514-5163 2019/02 [Refereed]
     
    This study aims to stabilize the resistance welding of carbon fiber reinforced thermoplastic (CFRTP) using spread or woven carbon fiber heating element. The joined CFRTP parts was sateen weave CF/PPS laminates, and the material used for the resistance heating element was spread carbon fiber and plain weave carbon fiber. The effects of processing conditions such as aspect ratio of fusion joining part, applied current, conduction time, and also material conditions such as resistance heating element were investigated experimentally. The contents of evaluation were temperature distribution of resistance heating element by using a thermography, welding area ratio measured by image analysis and monitoring of electricity. From the experimental results, in the case of width size change, it was suitable for resistance welding of large area. On the other hand, in the case of length size change, it was not suitable for resistance welding because the edge effect occurred around the electrode. Subsequently, in the case of using the spread carbon fiber as resistance heating element, it was found that the thermal distribution was unevenness because of uneven distribution of carbon fibers.
  • TANABE Daiki; IMAMURA Shota; NISHIYABU Kazuaki; KURASHIKI Tetsusei
    Transactions of the JSME (in Japanese) The Japan Society of Mechanical Engineers 82 (843) 16 - 00115-16-00115 2016 [Refereed]
     

    Automated thermoplastic tape laying (ATL) and automated fiber placement (AFP) are high-potential manufacturing methods for continuous carbon fiber reinforced thermoplastic (CFRTP) composites which can ensure operational safety even in highly loaded components such as aircraft wing skins and fuselages or construction large scaled structures. This study aimed to reveal the heating behavior of CFRTP in continuous tape layup molding. The material used for the experiment was unidirectional carbon fiber reinforced polyamide 6 (CF/PA6) prepreg tape. The effects of processing conditions such as output of infrared heater, feed speed of prepreg tapes and heating temperature of pressure rollers on the tape laying behavior of prepreg tape were investigated. In the case of only near infrared heating, it was revealed that the difference in temperature between the upside and downside prepreg tape was increased significantly. Then, the joining strength was decreased significantly compared with using the infrared heater, because the moisture in the prepreg tapes was not removed completely. On the other hand, when the near infrared heater and heating roller were used, the difference in temperature between the upside and downside prepreg tape was decreased considerably. It was also revealed that the surface temperature of CF/PA6 prepreg tape and singe lap tensile strength tends to increase with decreasing the feed speed of prepreg tapes.

  • Electro-fusion Joining of CF/PPS Composites using Carbon Fiber Heating Elements
    TANABE Daiki; NISHIYABU Kazuaki; KURASHIKI Teltusei
    Proceedings of the JSME/ASME 2014 International Conference on Materials and Processing (ICMP2014) 2014/06 [Refereed]
  • Daiki Tanabe; Kazuaki Nishiyabu; Tetsusei Kurashiki
    Zairyo/Journal of the Society of Materials Science, Japan Society of Materials Science Japan 63 (5) 368 - 373 1880-7488 2014 [Refereed]
     
    This study aims to reveal the mechanism of melting and oxidation phenomenon of CF/PPS laminated composites by electrically-conducting. The materials used are unidirectional CF/PPS and woven CF/PPS laminates. The effects of applied voltage, conducting time and fiber reinforcing configuration on melting behavior of CFRTP composites were investigated. The melting state was evaluated by microscopic observation and its image analysis. The experimental results revealed that the melting and oxidation behavior were influenced by reinforcing configuration and electric resistivity of CFRTP laminates. The melting area of both CFRTP laminates tends to increase with increasing the applied voltage and conducting time. It was found that the insertion of PPS films in melting interface was required in order to prevent the edge effect and non-uniform profile shapes of the melting area. It was also confirmed that woven CF/PPS laminates could be melted at low applied voltage. © 2014 The Society of Materials Science, Japan.
  • NISHIYABU KAZUAKI; TANABE DAIKI; KANOKO YASUHIRO; TANAKA SHIGEO
    TRANSACTIONS OF THE JAPAN SOCIETY OF MECHANICAL ENGINEERS Series A (Web) 79 (807) WEB ONLY 1593-1603  1884-8338 2013 [Refereed]
  • Kazuaki Nishiyabu; Daiki Tanabe; Yasuhiro Kanoko; Shigeo Tanaka
    Nihon Kikai Gakkai Ronbunshu, A Hen/Transactions of the Japan Society of Mechanical Engineers, Part A Japan Society of Mechanical Engineers 79 (807) 1593 - 1603 0387-5008 2013 [Refereed]
     
    This study aims to reveal the behavior of debinding and sintering in metal powder injection molding (MIM) process using copper powders with varied particle sizes. The feedstock composed of micron- and submicron-sized copper powders and polyacetal-based binder was adequately prepared. Oxidation process was added between debinding and sintering steps for decarburizing. The effects of processing temperature in debinding, oxidation and sintering were evaluated from the changes in weight, dimension, and residual carbon and oxygen contents in addition to microstructure. From the results obtained using micron- and submicron-sized copper powders, it was clarified that the oxidation conditions was very important for stably-obtaining the high dense sintered parts with lower carbon and oxidation contents. This is considered to be due to the mechanism that the binder was removed from green compacts at 873K in vacuum, and then copper oxide whiskers form on the surface of copper powder and grow to connect the particles each other by oxidizing in air. The experimental result showed that using submicron-sized powder could obtain the sufficient high dense sintered parts under low sintering temperature (973K). © 2013 The Japan Society of Mechanical Engineers.
  • Masaki Kotani; Kazuaki Nishiyabu; Satoru Matsuzaki; Shigeo Tanaka
    JOURNAL OF THE CERAMIC SOCIETY OF JAPAN CERAMIC SOC JAPAN-NIPPON SERAMIKKUSU KYOKAI 119 (1391) 563 - 569 1882-0743 2011/07 [Refereed]
     
    A simple method for making a porous SiC body through a polymeric route at one firing processing was demonstrated by the sacrificial filler template approach. By incorporating sacrificial pore-forming plastic powder, PMMA microbeads, into liquid preceramic polymer, AHPCS, and losing it after the polymer was hardened, a preceramic porous body was formed. As a consequence of systematic examination of the effects of particle size and mixture ratio of the powder, an AHPCS-derived porous SiC body was reproducibly formed without critical crack initiation. It was enabled only when the polymer was sufficiently contained to make a strong skeletal structure with the sacrificial plastic particles closely distributed. The porous microstructure would contribute to efficient gas emission and uniform thermal shrinkage during polymer pyrolysis, which reduced internal pressure and crack-causing thermal stress. (C)2011 The Ceramic Society of Japan. All rights reserved.
  • Kazuaki Nishiyabu; Daiki Tanabe; Yasuhiro Kanoko; Shigeo Tanaka
    Nihon Kikai Gakkai Ronbunshu, A Hen/Transactions of the Japan Society of Mechanical Engineers, Part A 77 (780) 1378 - 1387 0387-5008 2011 [Refereed]
     
    This study aims to develop the manufacturing method of micro-structured parts by the metal powder injection molding (MIM) inserted micro-sacrificial plastic molds which were prepared by nano-imprint lithography (NIL) technique. In this process named NIL/μ-SPiMIM, the feedstock composed of nano-sized copper powder and polyacetal-based binder was adequately prepared and molded into polymethylmethacrylate films with fine line-scan structures, and the molded parts were sintered in a reductive gas atmosphere followed by solvent debinding of the films. The behavior in debinding and sintering was investigated by thermo-gravimetric analysis, carbon and oxygen analysis and SEM observation. The effects of sintering temperature on sintered density, shrinkage, and profile accuracy were evaluated systematically. It can be concluded that the manufacturing method named NIL/μ-SPMIM proposed in this study has great potential to produce precisely 3 dimensional complex metallic parts with fine micro-structures. © 2011 The Japan Society of Mechanical Engineers.
  • NISHIYABU Kazuaki; TANABE Daiki; KANOKO Yasuhiro; TANAKA Shigeo
    TRANSACTIONS OF THE JAPAN SOCIETY OF MECHANICAL ENGINEERS Series A 一般社団法人 日本機械学会 77 (780) 1378 - 1387 1884-8338 2011 [Refereed]
     
    This study aims to develop the manufacturing method of micro-structured parts by the metal powder injection molding (MIM) inserted micro-sacrificial plastic molds which were prepared by nano-imprint lithography (NIL) technique. In this process named NIL/μ-SPiMIM, the feedstock composed of nano-sized copper powder and polyacetal-based binder was adequately prepared and molded into polymethylmethacrylate films with fine line-scan structures, and the molded parts were sintered in a reductive gas atmosphere followed by solvent debinding of the films. The behavior in debinding and sintering was investigated by thermo-gravimetric analysis, carbon and oxygen analysis and SEM observation. The effects of sintering temperature on sintered density, shrinkage, and profile accuracy were evaluated systematically. It can be concluded that the manufacturing method named NIL/μ-SPiMIM proposed in this study has great potential to produce precisely 3 dimensional complex metallic parts with fine micro-structures.
  • Kazuaki Nishiyabu; Kenichi Kakishta; Shigeo Shigeo
    Nihon Kikai Gakkai Ronbunshu, A Hen/Transactions of the Japan Society of Mechanical Engineers, Part A Japan Society of Mechanical Engineers 76 (761) 75 - 80 0387-5008 2010 [Refereed]
     
    The manufacturing method of resist film insert metal powder injection molding (MIM) namely Resist/μ-SpiMIM process has been proposed. The resist film made of PMMA polymer with numerous micro-holes was used as micro sacrificial plastic mold (SP-mold). A novel molding machine which could achieve to mold without pelletizing was also used to produce the green compacts with a high efficiency in experiment by using a small amount of feedstock. The feedstock prepared by pure copper powders with various particle sizes was injection-molded into the SP-mold and the sintered parts with micro-pillar structure were produced after debinding and sintering process. The effects of particle size on density, shape-transcription and surface roughness of those sintered parts were discussed. The decreasing of particle size results in a marked improvements of surface roughness, transcription and dimensional variation of sintered parts.
  • Kazuaki Nishiyabu; Kenichi Kakishita; Shigeo Tanaka
    Nihon Kikai Gakkai Ronbunshu, A Hen/Transactions of the Japan Society of Mechanical Engineers, Part A Japan Society of Mechanical Engineers 76 (767) 996 - 1001 0387-5008 2010 [Refereed]
     
    In microminiaturization of metal injection molding, the use of finer metal powders is one of solutions for improving the dimensional accuracy and surface roughness of sintered products. This study aims to investigate the effects of micro/nano powder ratio on the properties of sintered parts in μ-MIM process. A novel experimental machine which can achieve to mold without pelletizing was used to produce the tiny specimens with high trial efficiency and a small amount of feedstock. Small dumbbell specimens were produced with changing the binder content and the fraction of micro/nano copper powders. The effects of nano copper powder addition on the tap density of mixed powder, the viscosity of MIM feedstock and the grain size, surface roughness and tensile strength of sintered parts were revealed.
  • Kazuaki Nishiyabu; Shigeo Tanaka
    Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy 56 (5) 268 - 273 0532-8799 2009/05 [Refereed]
     
    A microplanetary gears made of stainless steel has been developed by micro metal powder injection molding (μ-MIM) process. In this stud., the accuracy and the quality of ultra-compact planet gear (module: m = 0.07 m., number of teeth: z=24) was evaluated. Cross-sections of the gear teeth were observed with a digital microscope and dimensions of the teeth were measured with a digital image processing. The variations in dimensions and shape of gear teeth were systematically investigated for mol., green and sintered part., and heat treated ones. The accuracy classes of the ultra-compact planet gear were defined from four shape variations of gear teet., i.e. total runou., single pitch deviatio., accumulated pitch deviation and tooth profile deviation. The accuracy class was concluded as JIS N class seven which is a comparatively high precise levei for practical applications.
  • TAKANO Naoki; TACHIKAWA Hiroto; MIYANO Naoya; NISHIYABU Kazuaki
    Journal of Solid Mechanics and Materials Engineering The Japan Society of Mechanical Engineers 3 (3) 504 - 612 1880-9871 2009/03 [Refereed]
     
    Aiming at the practical use of polyethylene glycol (PEG) microneedles for transdermal drug delivery system (DDS), a testing apparatus for their insertion into cultured human skin has been developed. To simulate the variety of conditions of human skin, biaxial tension can be applied to the cultured human skin. An adopted testing scheme to apply and control the biaxial tension is similar to the deep-draw forming technique. An attention was also paid to the short-time setup of small, thin and wet cultured skin. One dimensional array with four needles was inserted and influence of tension was discussed. It was found that tension, deflection of skin during insertion and original curvature of skin are the important parameters for microneedles array design.
  • 西籔 和明
    日本材料学会「材料」 58 (1) 87 - 92 2009/01
  • Kazuaki Nishiyabu; Shigeo Tanaka
    Metal Powder Report Elsevier Ltd 63 (3) 28 - 32 1873-4065 2008 [Refereed]
     
    The jury would still appear to be out considering the benefits of nanotechnology in metal injection moulding. Japanese researchers built their own tiny table-top direct mixing injection moulding machine to put theory to the test.... © 2008 Elsevier Ltd. All rights reserved.
  • Accuracy Evaluation of Ultra-compact Gears Manufactured by The MicroMIM Process
    西籔和明; Ian Andrews; 田中茂雄
    Inovar Communications Ltd., Powder Injection Molding International 2 (4) 60 - 63 2008
  • K. Nishiyabu; S. Matsuzaki; S. Tanaka
    POROUS METALS AND METALLIC FOAMS: METFOAM 2007 DESTECH PUBLICATIONS, INC 2 (3) 137 - + 2008 
    A production method for micro-porous metal components has been developed by applying the powder space holder (PSH) method to metal powder injection molding (MIM) process. This paper deals with the liquid infiltration property of micro-porous metals produced by the PSH method. The material used is high-corrosion resistant austenitic stainless steel 316L, and the samples have micro-sized open porous structures with high specific surface area. The test apparatus for evaluating the liquid infiltration performance of the porous specimens was developed using analytical balance. From the weight change in liquid infiltration test, the factors affecting water absorption behavior of porous specimens were studied. The results of the infiltration rate were linked to some important characteristics of the porous specimens such as mean pore diameter, liquid and gas permeability and specific surface area measured by capillary flow porometry. The effects of pore size on the infiltration rate were between those of porous specimens with a single digit pm and 15 mu m in mean constricted pore diameter.
  • NISHIYABU Kazuaki; MATSUZAKI Satoru; KOTANI Masaki
    Transactions of the Japan Society of Mechanical Engineers Series B The Japan Society of Mechanical Engineers 74 (743) 988 - 993 0387-5008 2008 [Refereed]
     
    The hybrid process, Polymer Impregnation and Pyrolysis combined with Powder Space Holder (PSH-PIP) method, has been newly developed to improve the reliability in structure and mechanical properties of SiC/SiC composite. This process can yield an open micro-porous structure derived from a precursor polymer which is ready for being densified by a subsequent PIP processing. Systematic experimental study has been done for the effects of the size and the fraction of the space holding particles on the microstructure. Consequently, SiC porous bodies without any significant cracks were successfully obtained by achieving efficient gas purge and homogeneous thermal shrinkage.
  • Kazuaki Nishiyabu; Satoru Matsuzaki; Shigeo Tanaka
    HIGH TEMPERATURE MATERIALS AND PROCESSES FREUND PUBLISHING HOUSE LTD 26 (4) 257 - 267 0334-6455 2007 [Refereed]
     
    A novel production method for the metal components with micro-sized porous structures has been developed by applying the powder space holder (PSH) method to the metal powder injection molding (MIM) process. This production method is compatible with widespread applications with high functionality such as heat sinks, electrodes and medical implants and so on. These applications can benefit from the advantages provided by micro-porous metal components with complicated shapes using most kinds of metal powder. The aim of this study is to clarify the effects of material combinations and production conditions on the pore formation and some physical properties of sintered porous metals. The green compacts were molded via uniaxial hot pressing for an experiment using various porous compounds which were prepared by changing the combinations in size of stainless steel 316L powder and polymethylmethacrylate (PMMA) space holding particle. Afterwards they were sintered at various temperatures after thermal debinding. It was confirmed that the size of metal powder and space holding particle together with the sintering temperature were main factors affecting the pore size, porosity, surface area ana shrinkage of sintered porous metals. It was concluded that the PSH-MIM method proposed was useful for producing metal components with micro-sized and high functionally porous structures.
  • Kazuaki Nishiyabu; Satoru Matsuzaki; Shigeo Tanaka
    PROGRESS IN POWDER METALLURGY, PTS 1 AND 2 TRANS TECH PUBLICATIONS LTD 534-536 981 - + 0255-5476 2007 [Refereed]
     
    A novel production method for porous metal components has been developed by applying powder space holder (PSH) method to metal powder injection molding (MIM) process. The PSH-MIM method has an industrial competitive advantage that is capable of net-shape manufacturing the micro-sized porous metal products with complicated shapes and controlled porosity and pore size. In this study, the small impeller with homogeneous micro-porous structure was manufactured by the PSH-MIM method using porous compounds composed of fine stainless steel 316L powder and polymethylmethacrylate (PMMA) particle. The effects of combinations in size and fraction of PMMA particle on dimensional tolerance and variation of sintered porous specimens were investigated. It was concluded that the PSH-MIM method could manufacture commercially micro-porous metal components with high dimensional accuracy.
  • Kazuaki Nishiyabu; Kenichi Kakishita; Shigeo Tanaka
    PROGRESS IN POWDER METALLURGY, PTS 1 AND 2 TRANS TECH PUBLICATIONS LTD 534-536 381 - + 0255-5476 2007 [Refereed]
     
    This study aims to investigate the effects of hybrid micro/nano powders in a micro metal injection molding (mu-MIM) process. A novel type of mixing-injection molding machine was used to produce tiny specimens (< 1 min in size) with high trial efficiency using a small amount of feedstock (< 0.05 cm(3) in volume). Small dumbbell specimens were produced using various feedstocks prepared by changing binder content and fraction of nano-scale Cu powder (130nm in particle size). The effects of adding the fraction of nano-scale Cu powder on the melt viscosity of the feedstock, microstructure, density and tensile strength of sintered parts were discussed.
  • Kazuaki Nishiyabu; Yasuhiro Kanoko; Shigeo Tanaka
    PROGRESS IN POWDER METALLURGY, PTS 1 AND 2 TRANS TECH PUBLICATIONS LTD 534-536 369 - + 0255-5476 2007 [Refereed]
     
    The production method of micro sacrificial plastic mold insert metal injection molding, namely mu-SPiMIM process has been proposed to solve specific problems involving the miniaturization of MIM. The sacrificial plastic mold (SP-mold) with fine structures was prepared by injection-molding polymethylmethacrylate (PMMA) into Ni-electroform, which is a typical LIGA ((L) under bar ithographie-(L) under bar alvanoformung-(L) under bar blonnLing) process. Stainless steel 316L feedstock was injectionmolded into the SP-mold which had micro structures with multi-pillars. The green compact was demolded as one component with the SP-mold, which was decomposed along with binder constituent of feedstock in debinding process. This study focused on the effects of metal particle size and processing conditions on the shrinkage, transcription and surface roughness of sintered parts, which were evaluated by SEM (Scanning Electron Microscope) observation.
  • Toshiko Osada; Hideshi Miura; Takanobu Yamagami; Kazuaki Nishiyabu; Shigeo Tanaka
    PROGRESS IN POWDER METALLURGY, PTS 1 AND 2 TRANS TECH PUBLICATIONS LTD 534-536 361 - + 0255-5476 2007 [Refereed]
     
    Gas surface treatment is considered to be especially effective for Titanium because of its high reactivity. In this study, we investigated the gas nitriding mechanism in titanium sintered parts produced by metal powder injection molding (MIM) process. In MIM process, gas nitriding can be surface-treated subsequently after debinding and sintering process. Then, the microstructure and nitrogen content of sintered MIM parts are considered to be greatly influenced by not only nitriding conditions but also sintered conditions. In this study, the effects of sintering time on microstructure such as nitrided layer thickness and hardness was investigated. Focus was given to the effects of specimen size on nitriding process, because the size of micro metal injection molding (mu-MIM) product is so small and the specific surface of that product is so large that the mechanical and functional properties can be subject to change by nitriding.
  • Kazuaki Nishiyabu; Satoru Matsuzaki; Shigeo Tanaka
    Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy 53 (9) 776 - 781 0532-8799 2006/09 [Refereed]
     
    A production method for porous metal components has been developed by applying powder space holder (PSH) method to metal powder injection molding (MIM) process. The PSH-MIM method has an industrial advantage which is capable of net-shape manufacturing the micro-size porous metal products with complicated shapes and controlled porosity and pore size. In this study, a small impeller made of stainless steel 316L was manufactured by injection molding, and a plate specimen was produced by extrusion molding to evaluate the dimensional accuracy of the porous sintered parts produced by the PSH-MIM method. The effects of combinations of size and fraction of space holder particle on the dimensional deviation and its coefficient of variance were investigated. It was concluded that the PSH-MIM method could manufacture commercially micro-porous metal components with high dimensional accuracy.
  • Toshiko Osada; Shigeo Tanaka; Kazuaki Nishiyabu; Hideshi Miura
    Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy 53 (9) 745 - 749 0532-8799 2006/09 [Refereed]
     
    In this study, gas nitriding was performed to various sizes of Titanium parts which were produced by metal injection molding (MIM) process, in order to add the high functionality with low processing cost. It was shown from the experiments that the nitriding treatment was useful for increasing the hardness of the surface which microstructure changed to the TiN and acicular α-Ti phase. With respect to the effect on the size of parts, micro dumbbell specimen had around five times higher content of nitrogen than block ones. It was suggested that the size of μ-MIM products is so small that the surface treatment contribute significantly and easily to improve the properties, especially gas nitriding process is one of effective surface treatment methods for high functionality of μ-MIM products.
  • K Kameo; K Nishiyabu; K Friedrich; S Tanaka; T Tanimoto
    WEAR ELSEVIER SCIENCE SA 260 (6) 674 - 686 0043-1648 2006/03 [Refereed]
     
    The wear resistance of stainless steel parts, which were fabricated by a metal injection molding (MIM) process, was studied under self-mating, dry sliding conditions, using a pin-on-disk type wear configuration. The materials used were an austenitic stainless steel 316L (of MIM and wrought steel), a precipitated stainless steel 174PH (of MIM and wrought steel) and a widely used ball-bearing steel (DIN 100Cr6). Two surface conditions, i.e. as sintered and as polished, were considered in the wear tests of the MIM samples. In summary, the wear resistance of 316L was lower than 17-4PH, and the latter was almost the same as 100Cr6. Further, the wrought materials showed a better wear resistance than the MIM materials. The mechanisms responsible for these tendencies were discussed by means of microscopical observations and chemical inspections of the worn surfaces and the microstructures of the samples. (c) 2005 Elsevier B.V. All rights reserved.
  • 西藪 和明; 柿下 健一; 鹿子 泰宏
    日本ばね学会 ばね論文集 日本ばね学会 (51) 55 - 62 0385-6917 2006
  • Toshiko Osada; Kazuaki Nishiyabu; Satoru Matsuzaki; Shigeo Tanaka; Hideshi Miura
    Nihon Kikai Gakkai Ronbunshu, A Hen/Transactions of the Japan Society of Mechanical Engineers, Part A 72 (713) 148 - 153 0387-5008 2006 [Refereed]
     
    Metal injection molding for tiny parts is called micro metal injection molding, " μ-MIM" which is considered to be one of promising process to manufacture the micro parts for various applications. In μ-MIM, the feedstock properties, particularly particle size and shape of metal powder are significantly important for the quality of micro parts. The purpose of this study is to investigate the effect of metal powder characteristics on the compactibility and sinterability. The three types of powders (3 μm and 9 μm water-atomized powders and 3 μm gas atomized powder) were used for the comparison. The melt viscosity of the feedstock was utilized as an index for evaluation of compactibility by injection moding. Then the spring shape of green compact specimen was produced by the micro injection molding machine. The green density was also evaluated for compactibility of the feedstock. The density and grain size of sintered specimens were investigated by changing sintering temperature and time.
  • Toshiko Osada; Shigeo Tanaka; Kazuaki Nishiyabu; Hideshi Miura
    Euro PM 2006 - Powder Metallurgy Congress and Exhibition 2 111 - 116 2006 
    © Euro PM 2006 - Powder Metallurgy Congress and Exhibition. All rights reserved. In this study, one of the surface functionalization processes, nitriding, is applied to Titanium MIM parts. To investigate the effect of the specific surface on the nitriding state three types of specimens, with different thickness, were adopted to nitriding. The nitrogen content of nitrided samples was evaluated by weight increase. The nitrogen content of the specimens increased with an increase in the specific surface. Moreover, to clarify the effect of nitriding conditions on nitrogen content, the nitrogen partial pressure in the furnace was controlled. The nitrogen content of specimens nitriding under a higher nitrogen partial pressure was higher than that of specimens in lower pressure environment. Micro Vickers hardness of micro dumbbell specimen was higher than that of block specimen, because of large specific surface; the nitrogen content inside the micro dumbbell specimen is also higher than that of the block specimen.
  • 金属粉末射出成形のマイクロ化への挑戦
    田中茂雄; 西籔和明
    日本塑性加工学会誌「塑性と加工」 46 (538) 24 - 29 2005/11
  • デジタル画像処理技術を用いたテキスタイル複合材料の非接触ひずみ分布計測
    西籔 和明
    日本繊維機械学会誌 「繊維工学」 58 (2) 2005/01
  • K Nishiyabu; S Matsuzaki; K Okubo; M Ishida; S Tanaka
    FUNCTIONALLY GRADED MATERIALS VIII TRANS TECH PUBLICATIONS LTD 492-493 (493) 765 - 770 0255-5476 2005 [Refereed]
     
    The production method for metal components with micro sized porous structure has been developed by applying "powder space holder method" to metal powder injection molding process. In this study, a co-sintering process was utilized to make a plate of sintered metal with micro porous graded structure, The green compact sheets with various contents of space hold particles were prepared by hot press molding for simplification. The five layers of metal with symmetric structure, which the skin layer was formed with high density metal and the core was formed with open or closed porous structure, or with inverse symmetry, was obtained by changing stacking sequence in co-sintering process. Mechanical properties of the materials with plain homogeneous porous structure and porous graded structure were compared. The usefulness of proposed method for producing the metal components with micro porous graded structure and the effective of graded structure to compensate the deficiencies on the mechanical property of porous metals was shown.
  • Satoru Matsuzaki; Shigeo Tanaka; Kazuaki Nishiyabu
    Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy Journal of the Japan Society of Powder and Powder Metallurgy 52 (1) 55 - 59 0532-8799 2005 [Refereed]
     
    This study aims to investigate the possibility for producing micro metal structured parts by applying micro metal injection molding (μ-MIM), the insert μ-MIM methods based on LIGA process were proposed, which used two types of sacrificial molds for MIM processing as following 1) PMMA (polymethylmethacrylate) resist and 2) PMMA mold injected in Ni electroformed mold. These processes were named "LIGA/μ-iMIM method" and the feasibility was checked by using SUS316L stainless steel powders. It was demonstrated that this method had a great potential to produce micro metal structured parts, also confirmed that the finer metal powders were better for their transcription than the coarse one.
  • デジタル画像処理技術を用いたテキスタイル複合材料の非接触ひずみ分布計測
    日本繊維機械学会誌「繊維工学」 58 (2) 2005
  • K Nishiyabu; S Matsuzaki; S Tanaka
    Sandwich Structures7: Advancing with Sandwich Structures and Materials SPRINGER 733 - 742 2005 [Refereed]
     
    This study describes the manufacturing method based on metal powder injection moulding for micro porous metal components with high functionally graded sandwich structure. The effectiveness of sandwich structure produced by co-sintering and co-injection moulding processes to compensate the deficiencies on the mechanical property of porous structures, was investigated.
  • K Okubo; S Tanaka; N Oya; K Nishiyabu; T Yanagisawa; M Tomita
    SANDWICH STRUCTURES7: ADVANCING WITH SANDWICH STRUCTURES AND MATERIALS SPRINGER 743 - 752 2005 [Refereed]
     
    This study describes the manufacturing method and physical properties of sandwich structure tubes using cup-stacked carbon nanotube/polypropylene and polypropylene. The effectiveness of sandwich structure produced by sequential injection moulding to enhance the axial and transverse compressive properties of thermoplastics was investigated. It was shown that compressive properties of the sandwich tubes effectively improved by proportionally positioning rich nanotube materials to the outer layer.
  • N Takano; M Zako; R Fujitsu; K Nishiyabu
    COMPOSITES SCIENCE AND TECHNOLOGY ELSEVIER SCI LTD 64 (13-14) 2153 - 2163 0266-3538 2004/10 [Refereed]
     
    The continuous fiber reinforced thermoplastic composites, such as textile composites, have many attractive properties and functions and they are used widely nowadays in industrial applications. The important point in the design and manufacturing is that the composites as well as the reinforcing textiles undergo large deformation during thermoforming, which is much influential on the overall properties. Hence, the large deformation characteristics must be investigated at thermoforming temperature. For this sake, the digital image-based measurement technique of large strain distribution is developed. It is applicable to arbitrary complex shaped components with the help of 3D-CAD. As the large strain definition, Biot's strain is adopted that is calculated by the polar decomposition of the deformation gradient tensor based on continuum mechanics. The developed strain measurement technique is applied to the deep-drawing of aramid rib-knitted fabric reinforced polypropylene composites. The comparison between rib and plain-knitted fabrics reinforced composites is studied and many differences are found. The large deformation characteristics are also investigated from microscopic point of view under uniaxial tension at thermoforming temperature. (C) 2004 Elsevier Ltd. All rights reserved.
  • Toshiko Osada; Kazuaki Nishiyabu; Satoru Matsuzaki; Shigeo Tanaka; Hideshi Miura
    Nihon Kikai Gakkai Ronbunshu, A Hen/Transactions of the Japan Society of Mechanical Engineers, Part A 70 (698) 1522 - 1528 0387-5008 2004 [Refereed]
     
    This study describes the micro evaluation methods for investigating the feedstock properties and the process conditions for industrial mass production of micro parts by Metal Injection Molding (MIM). The effects of feedstock properties such as particle size and powder loading on the sintered properties of micro-dumbbell specimens were investigated under various injection-molding conditions. Small particle size and high powder loading significantly improved the quality such as density and tensile strength, as well as yield percentage in producing sound micro-dumbbell sintered specimens. Deformation and fracture propagation behaviors were observed with the in-situ SEM tensile test which was useful to comprehend the influences of feedstock properties on the mechanical properties of the micro MIM (μ-MIM) products.
  • Toshiko Osada; Kazuaki Nishiyabu; Yasuo Karasaki; Shigeo Tanaka; Hideshi Miura
    Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy Journal of the Japan Society of Powder and Powder Metallurgy 51 (6) 435 - 440 0532-8799 2004 [Refereed]
     
    Producing the micro size parts by Metal Injection Molding (MIM) needs more sophisticated technique than the conventional injection molding. Especially, inhomogeneous state of the feedstock will strongly influence on the quality of the final products. In order to evaluate the mixing and palletizing conditions of the feedstock, statistical variations of density and binder contents in individual pellet were investigated by the weight measurement. These variations were discussed with coefficient of variation. The micro dumbbell specimens were fabricated using the feedstock, and the density and strength were investigated. Moreover, in order to improve the feedstock properties, re-pelletizing was performed. It was found that the homogeneity of the pellet was one of the important factors for quality of the micro size parts produced by MIM.
  • Surya D. Pandita; Kazuaki Nishiyabu; Ignaas Verpoest
    Composite Structures 59 (3) 361 - 368 0263-8223 2003 [Refereed]
     
    A strain mapping technique, namely digital photogrammetry, was used to investigate the tensile strain field of woven fabric composites in the presence of stress concentrations caused by geometrical defects consisting of circular or elliptical holes. Plain woven fabrics were used. The strain mapping technique clearly revealed the strain concentrations near the singularity. The strain concentrations are influenced by the tensile loading direction and the hole dimension relative to the size of the unit cell of the plain woven fabrics. A preliminary comparison of stresses approximately calculated from the strain field and theoretical stresses calculated from existing models such as Lekhnitskii's model is also presented. © 2003 Elsevier Science Ltd. All rights reserved.
  • TAKANO Naoki; ZAKO Masaru; FUJITSU Reiko; NISHIYABU Kazuaki
    Journal of the Japan Society for Composite Materials JAPAN SOCIETY FOR COMPOSITE MATERIALS 29 (1) 17 - 23 0385-2563 2003 [Refereed]
     
    Textile composite materials have large deformation characteristics, which leads to the superior formability. However, the large deformation of the textile preform is very much influential on the properties of the molded composite components. Hence, this paper aims at the measurement of large strain distribution in the complex shaped molded components of textile composites. A novel digital image-based procedure is proposed. The Green-Lagrange strain tensor is employed to express the large strain exactly and to avoid the misestimation due to the unmeasureable rotational motion during the closed molding. In pursuit of this, the deformation gradient tensor is calculated by the digitized information from the lattice pattern image drawn on the molded component. The proposed method is demonstratively applied to the deep-drawn components of rib-knitted fabric thermoplastic composites.
  • Yasutomo Uetsuji; Masaru Zako; Kazuaki Nishiyabu
    Zairyo/Journal of the Society of Materials Science, Japan Society of Materials Science Japan 51 (10) 1147 - 1153 0514-5163 2002 [Refereed]
     
    Although woven fabric composite materials have high performance, it is very difficult to reveal their mechanical behaviours due to the geometric complexity by theoretical analysis. Especially under damage development, several kinds of failure mode such as matrix cracking, fiber breaking and transverse cracking in fiber bundle affect the mechanical behaviour strongly. In order to analyze the mechanical behaviour, three-dimensional finite element analytical procedure based on damage mechanics has been developed. In this paper, the developed procedure is applied to plain woven fabric composites, and the mechanical behaviour under damage development by on-axis tensile load has been analyzed. On the other hand, on-axis tensile test has been performed in SEM and the change development at the edge cross-section of specimen has been observed. As a result, it can be confirmed that the calculational and the experimental results have a good agreement. Then, the mechanical behaviour depends on the edge effect of free side surface. Therefore the effect of free edge has been evaluated quantitatively by numerical analysis from comparison with mechanical behaviour under periodic boundary condition without free side surface. From the above results, it is recognized that the proposed procedure is very useful for the material design of woven fabric composite materials.
  • Mechanical and Antibacterial Properties of Copper-added Austenitic Stainless Steel (304L) by MIM
    Journal of Korean Powder Metallurgy Institute 9 (4) 227 - 234 2002 [Refereed]
  • Yooshikazu Masai; Masashi Ishida; Shigeo Tanaka; Kazuaki Nishiyabu
    Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy Funtai Funamtsu Yakin Kyokai/Japan Soc. of Powder Metallurgy 49 (9) 834 - 840 0532-8799 2002 [Refereed]
     
    The effect of copper-added content and sintering temperature on the mechanical properties and functional performances such as anti-bacteria and resist-corrosion for the stainless steel by metal injection molding was investigated. The specimens were prepared by injection molding the mixed powders of water-atomized SUS304L and Cu with poly-acetyl binder. The green compacts were prepared at five steps of copper-added content from 0mass%Cu to 5mass%Cu and they were sintered at the six steps of temperature from 1050 to 1350°C for 7.2ks in Ar gas after the debinding process at 600 °C for 7.2 ks in N2 gas. The relative density and tensile strength of sintered compacts showed the minimum values by addition of 5mass%Cu and 8mass%Cu, respectively. They were modified up to original value by addition of 10mass%Cu and sintering at 1100°C. The anti-bacterial test based on film contact to bacilli and the quantitative analysis of copper ion dissolved to water showed high effective as increasing the copper-added content. It was also confirmed from the measurement of pitting potential that copper addition modifies the resist-corrosion performance.
  • Naoyuki Oya; Kazuaki Nishiyabu; Hiroyuki Hamada
    Zairyo/Journal of the Society of Materials Science, Japan Society of Materials Science Japan 51 (5) 483 - 488 0514-5163 2002 [Refereed]
     
    This paper describes experimental developments for a concise preparation method of flexible interphase in commonly used GFRP and determination methods of the finite interphase thickness. The preparation scheme of the flexible interphase basically comprises surface coating of glass fibres with toughened epoxy resin. The finite thickness of the flexible interphase is determined by means of scanning electron microscopy equipped with energy dispersive X-ray element analyser and visco-elasticity image analysis featured in a scanning probe microscope. Certain evidences are successfully observed for the flexible interphase to be created by means of the proposed preparation method. However, it is found that the interphase thickness obtained from each method exhibits different values due to the particular sample status. The model composite used in the X-ray method contains a platinum layer as a boundary-indicator between the flexible interphase and the matrix resin. The platinum layer may hinder the interacting diffusion between the interphase and the matrix during the curing process, and this probably causes the broader interphase to remain in the model composite used in the X-ray method. Both methods are found to be useful to evaluate the interphase thickness around the single glass-filament at the microscopic level. However, those results show relatively large scatters this means that more efforts are still needed to create the interphase uniformly around the glass fibres using more sophisticated surface treatment techniques.
  • N Takano; Y Ohnishi; M Zako; K Nishiyabu
    INTERNATIONAL JOURNAL OF SOLIDS AND STRUCTURES PERGAMON-ELSEVIER SCIENCE LTD 38 (36-37) 6333 - 6356 0020-7683 2001/09 [Refereed]
     
    Process simulation of fiber reinforced composite materials is an important research theme for the development of low-cost and advanced functional composite materials. This paper aims at the simulation of deep-drawing process of knitted fiber reinforced thermoplastics and its verification. The feature of the simulation is that the large deformation of the knitted microstructures can be traced everywhere in the deep-drawn product. The homogenization theory is applied to analyze the micro-macro coupled behaviors of the knitted fabric composite material. By employing a simplified nonlinear computational algorithm, the deep-drawing simulation was carried out on a personal computer. The predicted largely deformed microstructures were compared with the experimental results. The numerical results and experimental ones agreed quite well. This deep-drawing simulation requires us to prepare only the mechanical properties of the constituents, while it provides us all the necessary quantities such as the deformation, strain, stress and stiffness from both microscopic and macroscopic standpoints. (C) 2001 Elsevier Science Ltd. All rights reserved.
  • 西籔 和明
    日本複合材料学会誌 JAPAN SOCIETY FOR COMPOSITE MATERIALS 27 (1) 56 - 64 0385-2563 2001/01
  • TAKANO Naoki; OHNISHI Yoshihiro; NISHIYABU Kazuaki; ZAKO Masaru
    Journal of the Society of Materials Science, Japan The Society of Materials Science, Japan 50 (5) 461 - 467 0514-5163 2001 [Refereed]
     
    A novel computational method for deep-drawing simulation of composite materials has been proposed with taking a three-dimensional continuum mechanics approach. The most notable feature is the consideration of micro-macro coupling effects by the mathematical homogenization theory. The homogenized properties and the constitutive law are evaluated carefully using the three-dimensional microstructure model under the large deformation and biaxial loading conditions. In this paper, the knit reinforcement of aramid fiber is studied, which has very complex microstructure architecture. The polypropylene is used as the matrix. The newly developed deep-drawing simulation provides us the macroscopic deformation, strain, stress and stiffness distribution as well as the largely deformed microstructures in the deep-drawn product. The high-speed computing technique which has been developed in the previous report enables us to carry out the micro-macro coupled nonlinear analysis easily on the personal computer. The experimental work has also been conducted, and the largely deformed microstructures are compared between experiment and simulation. A good coincident was obtained, which implies the validity and reliability of the proposed computational method.
  • T Fukui; A Nakai; H Hamada; K Nishiyabu
    2001: A MATERIALS AND PROCESSES ODYSSEY, BOOKS 1 AND 2 SOC ADVANCEMENT MATERIAL & PROCESS ENGINEERING 46 2409 - 2420 0892-2624 2001 [Refereed]
     
    In this study, reinforcement and matrix derived from the same kind of thermoplastics were used for polymorphism composite materials. The advantage of this material is not needed to take a chemical micmatch in adhesion into accout because the active cohesive force acts in the interface between fiber and matrix. The concept of such a material combination in composites can be applied for many kinds of thermoplastic materials. In this paper, Weft-knitted Polyethylene fabric reinforced Polyethylene sheet (namely, PE/PE sheet) was prepared by film stacking method. The effects of mold temperature in film stacking process on mechanical properties of PE/PE sheet were investigated. Injection molding specimens were prepared by inserting the PE/PE sheet, and low-density Polyethylene was used as matrix for injection molding, Mechanical properties of PE/PE injection composites were investigated. The tensile strength of PE/PE composites was higher than that of only PE matrix. The experimental results give evidence of the strong interface in PE/PE composite. In addition, the volume fraction of knitted fabric injection composite was only 4%, nevertheless the reinforcing efficiency is surprisingly high for the low fraction of reinforcement.
  • N. Takano; Y. Ohnishi; M. Zako; K. Nishiyabu
    International Journal of Solids and Structures Elsevier Science Ltd 37 (44) 6517 - 6535 0020-7683 2000 [Refereed]
     
    In order to analyze the mechanical behaviors of composite materials under large deformation, the formulation of the homogenization method is described. In this formulation, assuming that the microstructures in a local region of the global structure are deformed uniformly and that consequently the microscopic periodicity remains in the local region under large deformation, the microscopic deformation is precisely defined by the perturbed displacement and product of macroscopic displacement gradient and microscopic coordinates. Finally, microscopic and macroscopic equations are obtained. The above mentioned assumption of the periodicity of microstructures is experimentally validated. The computer program is also developed according to this formulation, and the large deformation is analyzed for the unidirectional fiber reinforced composite material and the knitted fabric composite material.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Soc Mater Sci, Japan 48 (5) 446 - 453 0514-5163 1999 [Refereed]
     
    The embedded single fiber transverse tensile test has been proposed as a new experimental evaluation method on composite interfaces. The effect of surface treatment on microscopic damage, such as the interfacial debonding and matrix cracking around a fiber was investigated by in-situ SEM observation, when the transverse tensile load to the fiber longitudinal direction was applied to an embedded single fiber composite. The experimental result revealed that the surface treatment condition of fibers has an influence on the initiation and propagation of interfacial debonding and matrix cracking around a single fiber. In addition, the effect of interfacial properties on microscopic damage was investigated by a finite element analysis. The analysis was carried out by using a three layers model, which was modeled separately, fiber, matrix and interphase into the test specimen. The property for the interphase was assumed to be orthotropic, i.e. both tensile and shear moduli of the interphase are dealt independently to express the role of interphase for stress bearing and stress transfer separately. The effect of interphase properties was investigated by changing the tensile and shear moduli of the interphase. The reasonable elastic properties of the interphase were obtained by comparing the computational results with experimental ones. The Hoffman's failure criterion was used for judging of the damage in the interphase and the matrix. The validity of this analytical method is verified by comparing the analytical results with the experimental ones.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Soc Mater Sci, Japan 48 (5) 430 - 437 0514-5163 1999 [Refereed]
     
    The effect of interfacial properties on damage behaviors of woven cloth fabric reinforced composites has been investigated by the edge cross-sectional observation of laminate under the tensile load in SEM. Test specimen used is vinyl ester resin matrix laminated composite reinforced by glass woven cloth. It is obvious that the surface treatment conditions of the fiber have affected the appearance of microscopic damages, such as the interfacial debonding and matrix cracking into the fiber bundle, or the generation of AE event. In the case of the fiber treated with the silane-coupling agent suitable for the matrix resin, only a few cracks occur into the fiber bundle just prior to the maximum load, and AE events generate fewer. In the case of chemical-mismatch treated fiber or non-treated fiber, however, much more cracks occur into the fiber bundle at the lower tensile load, but the generation behavior of AE events differs with each other. It is found by in-situ SEM observation that the fiber surface treatments have affected the initiation and progression of microscopic damage under the tensile load. Thus, it can be concluded that in-situ SEM observation with measuring both tensile load and AE event count is a useful evaluation method for understanding the effect of interfacial property on microscopic damage behavior.
  • FUJII Yoshimichi; NISHIYABU Kazuaki
    Journal of the Japan Society for Composite Materials JAPAN SOCIETY FOR COMPOSITE MATERIALS 25 (3) 95 - 101 0385-2563 1999 [Refereed]
     
    The objective of this investigation is to estimate the creep life of glass fiber reinforced plastic (GFRP) under stress-corrosive environments using acoustic emission (AE). The laminates were fabricated using combinations of vinylester resin (R806) and random fiber mat or woven cloth. The creep tests were conducted in 5% nitric acid (HNO3) environment. The AE depends on the loading level and the environment condition. For the creep test, the woven cloth reinforced specimens gave higher number of AE counts than the random mat reinforced specimens. The creep life decreased with increasing creep stress, whereas the rate of AE counts increased with increasing creep stress. A linear relationship was found between the creep life and the AE count rate. Using the proposed equation, a prediction of the creep life of GFRP under corrosive environments would presumably be possible.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Soc Mater Sci, Japan 48 (5) 446 - 453 0514-5163 1999 [Refereed]
     
    The embedded single fiber transverse tensile test has been proposed as a new experimental evaluation method on composite interfaces. The effect of surface treatment on microscopic damage, such as the interfacial debonding and matrix cracking around a fiber was investigated by in-situ SEM observation, when the transverse tensile load to the fiber longitudinal direction was applied to an embedded single fiber composite. The experimental result revealed that the surface treatment condition of fibers has an influence on the initiation and propagation of interfacial debonding and matrix cracking around a single fiber. In addition, the effect of interfacial properties on microscopic damage was investigated by a finite element analysis. The analysis was carried out by using a three layers model, which was modeled separately, fiber, matrix and interphase into the test specimen. The property for the interphase was assumed to be orthotropic, i.e. both tensile and shear moduli of the interphase are dealt independently to express the role of interphase for stress bearing and stress transfer separately. The effect of interphase properties was investigated by changing the tensile and shear moduli of the interphase. The reasonable elastic properties of the interphase were obtained by comparing the computational results with experimental ones. The Hoffman's failure criterion was used for judging of the damage in the interphase and the matrix. The validity of this analytical method is verified by comparing the analytical results with the experimental ones.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Soc Mater Sci, Japan 48 (5) 430 - 437 0514-5163 1999 [Refereed]
     
    The effect of interfacial properties on damage behaviors of woven cloth fabric reinforced composites has been investigated by the edge cross-sectional observation of laminate under the tensile load in SEM. Test specimen used is vinyl ester resin matrix laminated composite reinforced by glass woven cloth. It is obvious that the surface treatment conditions of the fiber have affected the appearance of microscopic damages, such as the interfacial debonding and matrix cracking into the fiber bundle, or the generation of AE event. In the case of the fiber treated with the silane-coupling agent suitable for the matrix resin, only a few cracks occur into the fiber bundle just prior to the maximum load, and AE events generate fewer. In the case of chemical-mismatch treated fiber or non-treated fiber, however, much more cracks occur into the fiber bundle at the lower tensile load, but the generation behavior of AE events differs with each other. It is found by in-situ SEM observation that the fiber surface treatments have affected the initiation and progression of microscopic damage under the tensile load. Thus, it can be concluded that in-situ SEM observation with measuring both tensile load and AE event count is a useful evaluation method for understanding the effect of interfacial property on microscopic damage behavior.
  • FUJII Yoshimichi; NISHIYABU Kazuaki
    Journal of the Japan Society for Composite Materials JAPAN SOCIETY FOR COMPOSITE MATERIALS 25 (3) 95 - 101 0385-2563 1999 [Refereed]
     
    The objective of this investigation is to estimate the creep life of glass fiber reinforced plastic (GFRP) under stress-corrosive environments using acoustic emission (AE). The laminates were fabricated using combinations of vinylester resin (R806) and random fiber mat or woven cloth. The creep tests were conducted in 5% nitric acid (HNO3) environment. The AE depends on the loading level and the environment condition. For the creep test, the woven cloth reinforced specimens gave higher number of AE counts than the random mat reinforced specimens. The creep life decreased with increasing creep stress, whereas the rate of AE counts increased with increasing creep stress. A linear relationship was found between the creep life and the AE count rate. Using the proposed equation, a prediction of the creep life of GFRP under corrosive environments would presumably be possible.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Soc Mater Sci, Japan 47 (6) 612 - 617 0514-5163 1998 [Refereed]
     
    The general aim of this study is to establish the modeling technique of interphase, which is the interfacial region between fiber and matrix, and to investigate the effects of interphase properties on the stress transfer mechanism and the fracture behavior in single fiber pull-out test. The finite element analytical model, which was divided independently with each element of fiber, matrix and interphase, has been applied. The interphase was assumed as orthotropy, because it can be dealt with the stress transfer and the stress bearing separately. The influence of interfacial shear stiffness on stress transmissibility was evaluated by the stress transferred from fiber to matrix by passing through the interphase. Also the effects of thermal stress which occurred at post-curing of resin, and meniscus which formed at the edge between fiber and matrix surface were investigated by FEM. From the analytical results, the following points were obtained (1) the interphase shearing modulus strongly affected the interfacial stress transmissibility, (2) the degree of stress concentration occurring at matrix surface was varied by interphase shear modulus, meniscus size and thermal stress, (3) the meniscus size largely affects both a success of pull-out testing and an appearance of the interfacial properties.
  • K Nishiyabu; M Zako
    DESIGN AND MANUFACTURING OF COMPOSITES TECHNOMIC PUBL CO INC 141 - 148 1998 [Refereed]
     
    This study describes about how the fiber surface treatments are affected on both mesoscopic damages, such as interfacial debonding and matrix cracking in the embedded single fiber or strand, and macroscopic ones, such as inter-bundle delamination of woven fabric composites. The damage observations have been carried out under two types of tensile testing: (1) tensile test into scanning electron microscope (in situ SEM observation) and (2) universal tensile test (in situ macro observation). Test specimens are vinyl ester resin matrix embedded by single filament or strand, and reinforced by laminated woven cloth. In order to investigate the effects of interfacial properties, each specimen was fabricated using three types of surface treated fiber. It was obvious that the interfacial properties were able to be evaluated by in situ observation of each failure process, such as interfacial debonding, crack linking, and crack propagation. The effect of the fiber surface treatment on damages has been revealed in each scale level, i.e., filament, strand, and woven fabric.
  • K Nishiyabu; A Yokoyama; H Hamada
    COMPOSITES SCIENCE AND TECHNOLOGY ELSEVIER SCI LTD 57 (8) 1103 - 1111 0266-3538 1997 [Refereed]
     
    To investigate the effect of interfacial properties on stress transfer by a numerical approach, a finite element model has been used where the fiber, the matrix and the interphase were treated separately. When the interphase was assumed to be orthotropic, an influence of the interfacial shear stiffness on stress transfer was evaluated from the axial tensile stress transferred from the matrix to the fiber by passing through the interphase. The influence of fiber breakage and interfacial debonding or matrix cracking on the stress distribution has also been studied. When the shear stiffness of the interphase is greater than that of the matrix, a high stress concentration appears near the fiber break point. However this stress concentration disappears when the fiber breakage occurs together with interfacial debonding or matrix cracking. If was therefore suggested that the fiber fracture propagation mode might be changed by altering the shear stiffness of the interphase and by the existence of interfacial debonding or matrix cracking. Thus it was obvious that the proposed FE numerical approach and the concept of material constants of the composite interphase might be appropriate for investigating the influence of the interfacial properties on stress transfer. (C) 1997 Elsevier Science Limited.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Society of Materials Science Japan 46 (4) 335 - 342 0514-5163 1997 [Refereed]
     
    In order to investigate the effect of the interfacial property on stress transmissibility, the finite element analytical model in which fiber, matrix and interphase were divided independently into mesh elements has been applied. The interfacial region was assumed as orthotropy. The concept of orthotropy on the composite interphase is suitable for investigating the effects of stress bearing and stress transfer on mechanical behaviors. This paper deals with the study on the influence of the gradient interphase on the stress transfer. Either the axial tensile modulus or the shear modulus was varied gradually in the interphase. From the analytical results, it is concluded that the difference in gradient distribution of the interfacial tensile modulus or the interfacial shear modulus affected both the interfacial stress transmissibility and stress bearing in the interphase. Therefore, it is obvious that this numerical analytical modelling on composite interface is suitable for the numerical approach of fiber reinforced composites, because it is possible to represent separately stress transfer and stress bearing as the role of the interface/interphase.
  • K Nishiyabu; A Yokoyama; H Hamada
    COMPOSITES SCIENCE AND TECHNOLOGY ELSEVIER SCI LTD 57 (8) 1103 - 1111 0266-3538 1997 [Refereed]
     
    To investigate the effect of interfacial properties on stress transfer by a numerical approach, a finite element model has been used where the fiber, the matrix and the interphase were treated separately. When the interphase was assumed to be orthotropic, an influence of the interfacial shear stiffness on stress transfer was evaluated from the axial tensile stress transferred from the matrix to the fiber by passing through the interphase. The influence of fiber breakage and interfacial debonding or matrix cracking on the stress distribution has also been studied. When the shear stiffness of the interphase is greater than that of the matrix, a high stress concentration appears near the fiber break point. However this stress concentration disappears when the fiber breakage occurs together with interfacial debonding or matrix cracking. If was therefore suggested that the fiber fracture propagation mode might be changed by altering the shear stiffness of the interphase and by the existence of interfacial debonding or matrix cracking. Thus it was obvious that the proposed FE numerical approach and the concept of material constants of the composite interphase might be appropriate for investigating the influence of the interfacial properties on stress transfer. (C) 1997 Elsevier Science Limited.
  • Kazuaki Nishiyabu; Atsushi Yokoyama; Masaru Zako
    Zairyo/Journal of the Society of Materials Science, Japan Society of Materials Science Japan 46 (4) 335 - 342 0514-5163 1997 [Refereed]
     
    In order to investigate the effect of the interfacial property on stress transmissibility, the finite element analytical model in which fiber, matrix and interphase were divided independently into mesh elements has been applied. The interfacial region was assumed as orthotropy. The concept of orthotropy on the composite interphase is suitable for investigating the effects of stress bearing and stress transfer on mechanical behaviors. This paper deals with the study on the influence of the gradient interphase on the stress transfer. Either the axial tensile modulus or the shear modulus was varied gradually in the interphase. From the analytical results, it is concluded that the difference in gradient distribution of the interfacial tensile modulus or the interfacial shear modulus affected both the interfacial stress transmissibility and stress bearing in the interphase. Therefore, it is obvious that this numerical analytical modelling on composite interface is suitable for the numerical approach of fiber reinforced composites, because it is possible to represent separately stress transfer and stress bearing as the role of the interface/interphase.

Books etc

  • Handbook of metal injection molding
    NISHIYABU Kazuaki (Joint workPowder space holder metal injection molding (PSH-MIM) of micro-porous metals)Woodhead Publishing 2012/06
  • Some Critical Issues for Injection Molding
    NISHIYABU Kazuaki (Joint workMicro Metal Powder Injection Molding)InTech 2012/03
  • Recent Development in Research of Macro- and Nanoporous Metals
    中嶋英雄 (Contributor金属粉末射出成形によるマイクロポーラス金属精密部品の製造法)シーエムシー出版 2010/07
  • 「工業材料」2005年10月号,特集:傾斜機能材料-その魅力と応用事例
    西藪和明 (Joint workマイクロ多孔質構造が段階的に変化する傾斜機能多層金属の開発)日刊工業新聞社 2005/10 48-52頁 
    Vol.53 No.10
  • マイクロリアクタテクノロジー ~限りない可能性と課題~
    西籔和明 (Joint work金属粉末射出成形技術を用いたマイクロリアクタの製造)エヌ・ティー・エス 2005/07

Conference Activities & Talks

  • 田邉大貴; 倉敷哲生; 傳谷真司; 西籔和明
    日本複合材料合同会議(CD-ROM)  2013
  • 田邉大貴; 傳谷真司; 西籔和明; 倉敷哲生
    日本繊維機械学会年次大会研究発表論文集・講演要旨集  2013
  • 森椙哲也; 服部佑紀; 西籔和明
    日本複合材料合同会議(CD-ROM)  2013
  • 桜井晋也; JUSOH Mohd; Ikhwan Helmi; 西籔和明
    日本複合材料合同会議(CD-ROM)  2013
  • 田渕喜瑛; 西籔和明; 田邉大貴; 倉敷哲生
    日本複合材料合同会議(CD-ROM)  2013
  • 鹿子 泰宏; 西籔 和明; 田邉 大貴; 田中 茂雄
    日本機械学会第18回機械材料・材料加工技術講演会(M&P2010)  2011/11  東京大学  日本機械学会第18回機械材料・材料加工技術講演会(M&P2010)
     
    本研究は,焼結性が高く,寸法精度や表面粗度に優れたナノサイズの純銅粉末にダイヤモンド粒子を添加し,ダイヤモンドの熱劣化温度以下での焼結を試み,焼結体の熱伝導性を調査した.また,著者らがこれまでに金属粉末射出成形(Metal Injection Molding,MIM)技術を応用し,研究開発してきた微細な三次元構造体を製造するマイクロ犠牲樹脂型インサートMIM(Micro Sacrificial Plastic Mold Insert MIM,μ-SPiMIM)に銅/ダイヤモンド複合材を適用し,微細なピラー構造を有するマイクロヒートシンクの製造可能性を調査した.
  • ナノ銅粉末を用いたマイクロ高機能化プロセッシングの挑戦  [Not invited]
    西籔 和明
    (社)粉体粉末冶金協会,第22回 射出成形技術・評価研究会  2011/11  京都  (社)粉体粉末冶金協会,第22回 射出成形技術・評価研究会
     
    本講演では,ナノ銅粉末を用いた2つの先進的な製造法の開発についての取り組みを紹介する.1つは,ナノ銅粉末を用いたナノインプリント犠牲樹脂型インサートMIMによるマイクロ構造体の作製法であり,その脱脂・焼結過程について詳説する.もう1つは,超高性能マイクロヒートシンクの量産化を目的に開発したマイクロ犠牲樹脂型インサートMIMによる柱状構造を有するダイヤモンド粒子添加銅焼結体の作製法である.
  • 西籔 和明; 鹿子 泰宏; 田邉 大貴; 田中 茂雄
    PM2010 WORLD CONGRESS  2011/10  イタリア  PM2010 WORLD CONGRESS
     
    本研究は,ナノサイズの純銅粉末にダイヤモンド粒子を添加し,ダイヤモンドの熱劣化温度以下での焼結を試み,焼結体の熱伝導性を調査するとともに,マイクロ犠牲樹脂型インサート金属粉末射出成形(?-SPiMIM)プロセスを用いて,銅/ダイヤモンド複合材のマイクロヒートシンクの製造可能性を調査した結果について発表した.(英文)
  • 増永賢司; 西籔和明; 森本純司; 橋本知久; 田中茂雄
    日本機械学会年次大会講演論文集  2011/09
  • 西籔和明; 田邉大貴; 鹿子泰宏; 田中茂雄
    日本機械学会年次大会講演論文集  2011/09
  • 吉澤賢宏; 田邉大貴; 西籔和明; 倉敷哲生
    日本機械学会年次大会講演論文集  2011/09
  • 大久保健児; 田中茂雄; 伊藤浩志; 西籔和明
    日本機械学会年次大会講演論文集  2011/09
  • NISHIYABU Kazuaki
    Journal of the Society of Materials Science, Japan  2011
  • KURASHIKI Tetsusei; NISHIYABU Kazuaki
    Journal of the Society of Materials Science, Japan  2011
  • KANOKO Yasuhiro; TANAKA Shigeo; TANABE Daiki; NISHIYABU Kazuaki
    Materials and processing conference  2010/11 
    This study aims to develop the MIM process for manufacturing the micro heat sinks made of copper / diamond composites with high thermal conductivity. Diamond particles were added into the feedstock composed of copper powder and polyathetal-based binder. The compound feedstock was molded into sacrificial plastic mold (SP-mold), and the green compacts with micro-pillars were obtained and removed the SP-mold by solvent extraction. Nano-sized copper powder was used for drastically decreasing the sintering temperature to prevent from occurring thermal damages on the surfaces of diamond particles. The sintered parts were also prepared by spark plasma sintering in contrast with furnace sintering, and they were evaluated by density and thermal conductivity measurements. The experimental results showed that using nanopowder could obtain a sufficient high sintered density under low sintering temperature.
  • 西籔 和明; 田邉 大貴; 鹿子 泰宏; 田中 茂雄
    PM2010 WORLD CONGRESS  2010/10  イタリア  PM2010 WORLD CONGRESS
     
    本研究は,ナノサイズの純銅粉末を,ナノインプリントリソグラフィにより製造した犠牲樹脂型に射出成形し脱脂・焼結工程を経て精密なマイクロ構造体を得るNIL/μ-SPiMIMプロセスに適用し,射出成形条件および脱脂・焼結工程の最適条件の検討を行い,マイクロ構造体の製造の可能性を調査した結果について発表した.(英文)
  • 西籔 和明; 田邉 大貴; 鹿子 泰宏; 田中 茂雄
    日本材料学会複合材料部門委員会2010年度JCOM若手シンポジウム  2010/08  兵庫県豊岡市城崎町湯島1062  日本材料学会複合材料部門委員会2010年度JCOM若手シンポジウム
     
    本研究では,焼結性が高く,寸法精度や表面粗さに優れたナノサイズの純銅粉末にダイヤモンド粒子を添加し,ダイヤモンドの熱劣化温度以下での焼結を試み,焼結体の熱伝導性を調査した.加えて,著者らが金属粉末射出成形(Metal Injection Molding,MIM)技術を応用し開発した,微細な三次元構造体が製造可能なマイクロ犠牲樹脂型インサートMIM(Micro Sacrificial Plastic Mold Insert MIM,μ-SPiMIM)に銅/ダイヤモンド複合材を適用し,微細なピラー構造を有するマイクロヒートシンクの製造可能性を調査した.
  • 西籔 和明; 尾原 礼俊
    日本材料学会複合材料部門委員会2010年度JCOM若手シンポジウム  2010/08  兵庫県豊岡市城崎町湯島1062  日本材料学会複合材料部門委員会2010年度JCOM若手シンポジウム
     
    本研究は,これまで荷重下での一方向強化複合材料の弾性変形に対する計測および解析の精度に関して検証した報告はあまり見受けられないため,基礎研究に立ち帰り,繊維配向角の異なる一方向炭素繊維強化プラスチックに集中荷重を作用させた際に生じる片持ち曲げ変形挙動を接触式の三次元座標測定,非接触式の三次元変形解析システムを用いた実験および有限要素解析から調査した.また,実験および解析の結果を検証し計測精度を調査した.
  • KANOKO Yasuhiro; TANAKA Shigeo; TANABE Daiki; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2010  The Japan Society of Mechanical Engineers
     
    This study aims to develop the MIM process for manufacturing the micro heat sinks made of copper / diamond composites with high thermal conductivity. Diamond particles were added into the feedstock composed of copper powder and polyathetal-based binder. The compound feedstock was molded into sacrificial plastic mold (SP-mold), and the green compacts with micro-pillars were obtained and removed the SP-mold by solvent extraction. Nano-sized copper powder was used for drastically decreasing the sintering temperature to prevent from occurring thermal damages on the surfaces of diamond particles. The sintered parts were also prepared by spark plasma sintering in contrast with furnace sintering, and they were evaluated by density and thermal conductivity measurements. The experimental results showed that using nanopowder could obtain a sufficient high sintered density under low sintering temperature.
  • TANABE Daiki; NISHIYABU Kazuaki; KANOKO Yasuhiro; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2010  The Japan Society of Mechanical Engineers
     
    This study aims to reveal debinding-sintering process of the micro-structured parts by the metal powder injection molding (MIM) inserted sacrificial plastic molds which were prepared by thermal nanoimprint lithography (NIL). The microscopic transcriptional property in molded and sintered parts was evaluated by cross-sectional SEM observation. The experimental results revealed reasonable evidences that using nanopowder could sinter at very low temperature with keeping the fine shapes. It can be concluded that the manufacturing method of NIL/μ-SPiMIM has great potential to produce precisely metallic parts with a single-digit micrometered structures.
  • SUS316Lの脱バ・焼結過程に生じる諸現象  [Not invited]
    岩津 修; 西籔 和明; 田中 茂雄; 豊島 孝文
    粉体粉末冶金協会 射出成形技術・評価研究会  2010  粉体粉末冶金協会 射出成形技術・評価研究会
  • MUTO Masahiro; NISHIYABU Kazuaki; WATANABE Takashi
    Materials and processing conference  2009/11
  • OHARA Ayatoshi; NAKAO Yuki; NISHIYABU Kazuaki
    Materials and processing conference  2009/11
  • NISHIYABU Kazuaki
    The Reference Collection of Annual Meeting  2009  The Japan Society of Mechanical Engineers
  • NISHIYABU Kazuaki; TANABE Daiki; KANOKO Yasuhiro; Tanaka Shigeo
    The proceedings of the JSME annual meeting  2009  The Japan Society of Mechanical Engineers
     
    This study aims to develop the manufacturing method for micro-structured parts with sub-micron porous structure. MIM feedstock composed of nano-sized copper powder and polymeric binder was injection-molded into micro-sacrificial plastic mold (SP-mold) which was prepared by nano-imprint lithography (NIL) technique, and sintered at low temperature followed by solvent debinding of the SP-mold. It was shown from trial study that the micro-structured parts with sub-micron porous structure could be precisely obtained by the process named NIL/μ-SPiMIM developed in this study.
  • 粉末成形の基礎と素材製造プロセス 3.金属粉末射出成形の最近の進歩  [Not invited]
    西籔和明
    日本材料学会「材料」  2009
  • TAKANO Naoki; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2008  The Japan Society of Mechanical Engineers
     
    One of the authors has developed a novel manufacturing method of micro mechanical parts made of porous metals named powder space holder metal injection molding (SPH-MIM). This study presents an original numerical analysis of inner local stress considering the microstructure architecture by the finite element mesh superposition method, which aims at proposing the strength evaluation and design methodology for those micro parts. Fracture test, digital image-based measurement of macroscopic surface strain distribution and numerical results are presented in this paper.
  • Small is better if testing MIM nano theories  [Not invited]
    西籔和明; 田中茂雄
    Metal Powder Report  2008
  • NISHIYABU Kazuaki
    年次大会講演資料集  2007/09 
    The possibility of micro and high functional processings by metal powder injection molding (MIM) which uses effectively polymeric materials for enhancing both mold-ability and shape-retention were introduced. Sacrificial plastic mold inserted metal injection molding (SPiMIM) was developed to overcome some problems facing the realization of μ-MIM process. The molds were manufactured by LIGA process. Two types of transcription methods were adopted in LIGA/μ-SPiMIM process to obtain the sintered parts with multi pillars or fluidic channels. The effects of particle size on the quality of micro-structured parts were also investigated.
  • UEMURA Takeshi; TAKANO Naoki; MIYANO Takaya; OKANISHI Takaaki; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2007  The Japan Society of Mechanical Engineers
     
    This paper describes a hybrid evaluation technique of mechanical characteristics for the insertion of microneedles into cultured skin. The developed device applies uniform tension to cultured skin, the value of which is calculated by large deformation and viscoelastic finite element analysis. It has been confirmed that the microneedle made of polyethyleneglycol was saccessfuly inserted into cultured skin.
  • KOTANI Masaki; ZIMMER Aline; MATSUZAKI Satoru; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2007  The Japan Society of Mechanical Engineers
     
    As a promising approach to improve a matrix microstructure of SiC/SiC composite, the polymer impregnation and pyrolysis process combined with powder space holder technique (PSH-PIP) has been developed. PSH method was employed for making porous structure which potentially contributes to efficient gas purge and uniform shrinkage during pyrolysis. Under the best matrix producing condition which had been found through monolith productions, unidirectional SiC/SiC composites were successfully fabricated. By comparing them with a conventionally-fabricated composite, the matrix formation of improved homogeneity with smaller amount of process defects was certainly approved. The effectiveness of the microstructural improvement on mechanical properties was explicitly demonstrated as expected.
  • NISHIYABU Kazuaki; MATSUZAKI Satoru; KOTANI Masaki
    The proceedings of the JSME annual meeting  2007  The Japan Society of Mechanical Engineers
     
    This study aims to develop the heat-resistant composite materials with high reliability in strength. The adoption of powder space holder (PSH) method into polymer impregnation and pyrolysis (PIP) process was proposed to reduce predominant defects formed in the firing process of SiC precursor polymer. The effects of size and fraction of space holding particle made of polymethylmethacrylate on the pore formation behavior were mainly investigated. Consequently, SiC porous materials and the fibrous composite materials with homogeneous open porous structure were successfully obtained without significant defects. This is surely due to an efficient gas purge and a stable shrinkage by introducing the porous structure in SiC matrix.
  • MATSUZAKI Satoru; TANAKA Shigeo; NISHIYABU Kazuaki; OCHI Toshiaki
    The proceedings of the JSME annual meeting  2007  The Japan Society of Mechanical Engineers
     
    This study aims to evaluate the functional properties such as heat radiation performance and water absorption power of micro-porous metals produced by powder space holder method To investigate the effects of pore size on heat radiation performance, the heat transfer coefficients of micro-porous copper specimens were measured under various air flow rates. Also, to know the water absorption behavior of micro-porous metals, the weight change of porous stainless-steel specimens in a water immersion was evaluated.
  • MORIMOTO Kei; NISHIYABU Kazuaki; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    This study describes the methodology on fabrication and quality evaluation of me micro-gear manufactured by metal powder injection molding (MIM). Cross-sections of the gear teeth are observed with a digital microscope and dimensions of teethes were measured by an image analysis. The variation in dimensions of teethes in a piece of micro-gear and between micro-gears was compared. It was shown that those experiments contribute useful information on the quality of the micro gear.
  • YAMAGAMI Takanobu; NISHIYABU Kazuaki; OSADA Toshiko; TANAKA Shigeo; MIURA Hideshi
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    The general aim of this study is to develop the surface functionalization process in metal powder injection molding (MIM). A gas nitriding process which can improve the wear and corrosion resistances was investigated for sintered Ti and its alloy parts through the MIM process to realize the high functionality at low processing cost. The effects of the specimen size and the process conditions on the nitriding reaction in the Ti-6Al-4V MIM parts were mainly investigated by micro-structural observation and hardness measurements. The gas nitriding mechanisms were discussed. The results suggested that the gas nitriding process was a useful surface treatment process for high functionality of micro metal injection molding (μ-MIM) products.
  • NISHIYABU Kazuaki; KAMEO Koji; FRIEDRICH Klaus; TANIMOTO Toshio; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    The wear resistance of stainless steel parts, which were fabricated by a metal injection molding (MIM) process, was studied under self-mating, dry sliding conditions, using a pin-on-disk type wear configuration. The materials used were an austenitic stainless steel 316L (of MIM and wrought steel), a precipitated stainless steel 17-4PH (of MIM and wrought steel), and a widely used ball-bearing steel (DIN 100Cr6). Two surface conditions, i.e. as sintered and as polished, were considered in the wear tests of the MIM samples. In summary, the wear resistance of 316L was lower than 17-4PH, and the latter was almost the same as 100Cr6. Further, the wrought materials showed a better wear resistance than the MIM materials. The mechanisms responsible for these tendencies were discussed by means of microscopical observations and chemical inspections of the worn surfaces and the microstructures of the samples.
  • NISHIYABU Kazuaki; KANOKO Yasuhiro; Tanaka Shigeo
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    The aim of this study is to improve the quality of micro-structured parts manufactured by Micro Sacrificial Plastic Mold Inserted Metal Powder Injection Molding (μ-SPiMIM) process using LIGA. The defects in plastic injection molding such as weld-line and short filling, which developed around micro pillar structures of plastic molds, were evaluated with a laser microscope observation. The effects of molding conditions on the quality in micro injection molding of micro plastic parts were discussed. The effects of molding conditions in metal powder injection molding were also investigated.
  • NISHIYABU Kazuaki; HIRAO Hiroshi; MATSUZAKI Satoru; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    A novel production method for the metal components with micro-sized porous structures has been developed by applying powder space holder (PSH) method to metal powder injection molding (MIM) process. This method is capable of manufacturing with high dimensional accuracy the micro-porous metal components with complicated shapes using most kinds of metal powder. The size of metal powder and space holding particle in addition to sintered temperature are main factors affecting significantly for the pore size, porosity, surface area and shrinkage of sintered porous metals. The method proposed is useful in producing the graded porous structure for high functionally.
  • FUTAHASHI Yuki; NISHIYABU Kazuaki; MATSUZAKI Satoru; TANAKA Shigeo; KOTANI Masaki
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    This study aims to develop a heat-resistant composite material with high safety and reliability towards realization of re-use type space transportation system. Silicon carbide (SiC) which has high thermal conductivity and chemical inactive was adopted. To modify the brittleness of SiC, the micro-porous materials were produced by powder space holder (PSH) method. The production conditions of SiC porous materials and SiC fiber reinforced SiC porous composite material were considered. The problems of the heating process of SiC precursor polymer were solved by changing the particle size and the mixture ratio of pore formation materials. Consequently, SiC porous materials without crack with homogeneous open porous structure were obtained.
  • HIRAO Hiroshi; NISHIYABU Kazuaki; SHINAGAWA Kazunari; MATSUZAKI Satoru; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    A novel production method for the metal components has been developed by applying powder space holder (PSH) method to metal injection molding (MIM) process. Micro porous metals which have controlled closed or open pore structures are produced by PSH-MIM method. It is important for producing the products with high-quality to understand the effects of material combination and sintering temperature on pore size and porosity. The aim of this study is to investigate the effectiveness of the numerical analysis for their prediction. The analytical results showed the similar tendency to the experimental ones on sintering shrinkage of porous metals prepared using various volume fractions of space holding particle.
  • KAKISHITA Kenichi; NISHIYABU Kazuaki; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2006  The Japan Society of Mechanical Engineers
     
    Micro metal powder injection molding (μ-MIM) needs more sophisticated techniques than the conventional MIM. The use of finer powders is one of solutions to improve the dimensional accuracy and surface roughness of sintered products. This study aims to investigate the effectiveness of nano powder in μ-MIM process. To produce the tiny specimens with high trial efficiency and a small amount of feedstock, a novel experimental machine which can achieve to mold without pelletizing was used. Minute pattern specimens were produced with changing the binder content and the size of copper powder. The effects of particle size of metal powder on the tap density, melt viscosity, and surface roughness, microstructure of sintered parts were discussed.
  • OSADA Toshiko; MIURA Hideshi; TAKEMASU Teruie; UEMURA Makoto; NISHIYABU Kazuaki; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2005  The Japan Society of Mechanical Engineers
     
    In this study, gas nitriding was processed for various sizes of Titanium parts which were produced by metal injection molding (MIM) process, for the sake of enabling the high functionality at low processing cost. It was shown from the experiments that nitriding treatment resulted in increasing hardness on the surface and the microstructure changed to the TiN and acicular α-Ti phase. To effect on the size of parts, micro dumbbell specimen had around five times higher content of nitrogen than block ones. It is concluded that the size of μ-MIM products is so small that surface treatment can contribute significantly to improve the properties, and then gas nitriding process is one of effective surface treatment methods for high functionality of μ-MIM products.
  • NISHIYABU Kazuaki; KAKISHITA Kenichi; OSADA Toshiko; MATSUZAKI Satoru; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2005  The Japan Society of Mechanical Engineers
     
    Micro powder injection molding (μ-PIM) needs more sophisticated techniques than the conventional PIM The use of finer powders is one of solutions to improve the dimensional accuracy and surface roughness of sintered products. This study aims to investigate the effects of hybrid micro/nano powders on feedstock properties in μ-PIM process. To produce the tiny specimens with high trial efficiency and a small amount of feedstock, a novel experimental machine which can achieve to mold without pelletizing was used. Small dumbbell specimens were produced with changing the binder content and the fraction of nano-scale copper powder. The effects of nano-scale copper powder addition on the tap density of mixed powder, the viscosity of feedstock and microstructure of sintered bodies were discussed.
  • TAIRA Kensuke; TANAKA Shigeo; NISHIYABU Kazuaki; KANOKO Yasuhiro
    The proceedings of the JSME annual meeting  2005  The Japan Society of Mechanical Engineers
     
    The μ-MIM process using the sacrificial plastic mould (SP-mould), namely micro sacrificial plastic mould insert metal injection molding (μ-SPiMIM) method has been developed to solve the above-mentioned problems specific to μ-MIM, and to be freed from ordinary constraints of shapes. The SP-moulds are prepared by three types of methods; 1) machining, 2) LIGA process and 3) rapid prototyping for zigzag-shaped spring, multi-pillar and micro-impeller, respectively. This study aims to demonstrate the possibility of μ-SPiMIM process for producing the tiny and micro-structured parts, and to show the characteristics in production method of SP mould for μ-SPiMIM process.
  • OKUBO Kenji; TANAKA Shigeo; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2005  The Japan Society of Mechanical Engineers
     
    This study aims to develop processing techniques to improve dimensional accuracy of tiny parts produced by micro metal injection molding (μ-MIM). Micro dumbbell specimens were molded by a micro injection molding machine, which can be monitored with the mold pressure in injection process measured at the both side chucking portions. The effects of particle size distribution of stainless steel powders on the mold pressure and dimension in green compacts and sintered bodies were investigated. The reduction of the difference in dimension of chucking parts of micro dumbbell specimens to 5μm was achieved by using the powder undercut below 5μm in particle diameter.
  • 金属粉末射出成形のマイクロ化への挑戦  [Not invited]
    田中茂雄; 西籔和明
    日本塑性加工学会誌「塑性と加工」  2005
  • NISHIYABU Kazuaki; MATSUZAKI Satoru; ISHIDA Masashi; TANAKA Shigeo
    The proceedings of the JSME annual meeting  2004  The Japan Society of Mechanical Engineers
     
    The production method for metal parts with micro sized porous structure has been developed by applying "powder space-holder method" in metal powder injection molding process. In addition to metal powder and thermoplastic binders, coarse spherical material made of thermoplastic was used as lost material for formation of fine porous structures. The specimens were made by extrusion and injection moldings. The difference in these molding methods on the porous structure and those mechanical properties were investigated. It was shown that the porosity and strengths were controllable by changing the volume fraction of space holding particles. If was also demonstrated that the complicated shaped metal parts with micro porous structures can be produced using various kinds of metal powders by using metal injection or extrusion molding methods.
  • OKUBO Kenji; TANAKA Shigo; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2004  The Japan Society of Mechanical Engineers
     
    Micro Metal injection molding (μ-MIM) is one of premising processes to manufacture tiny metal parts. Micro dumbbell specimens were molded by a micro injection molding machine, the mold pressure in injection process was measured at the both side chucking portions, and the effects of injection volume on the mold pressure and dimension in green compacts and sintered bodies were investigated. Dimension of molded parts and sintered ones were correlated by injection volume and then the possibility for dimensional control by the mold pressure was shown. It was also confirmed that the micro injection machine has some advantages for producing μ-MIM products.
  • YUZUKI Akio; OSADA Toshiko; TANAKA Shigeo; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2004  The Japan Society of Mechanical Engineers
     
    In order to improve the variation in quality of tiny parts produced by micro Powder Injection Molding (μ-PIM) and to study the effects of compounding ratio and additives with a minute amount of materials, a new concept of small mixing and injection molding machine has been developed. This machine enabled to mix metal powder and binders followed by injection molding, therefore it can achieve to mold without pelletizing process, namely "pellet-less" injection molding. It has a small furnace to mix and plasticization when injection molding, plunger which works as a screw during mixmg and also plunger for injection molding. As a trial mixing and molding, it is confirmed that the pellet would be homogeneous in a certain mixing condition and the variation in density of micro dumbbell specimen was slight.
  • MATSUZAKI Satoru; TANAKA Shigeo; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2004  The Japan Society of Mechanical Engineers
     
    This study aims to investigate the possibility for producing microstructure metal parts by applying micro metal injection molding (μ-MIM) in molding process of LIGA. The micro insert MIM methods based on LIGA process were proposed, and used two types of sacrificial molds for MIM as following; 1) PMMA resist and 2) PMMA mold injected in Ni electroformed mold. These processes named "LIGA/μ-iMIM" and were realized using SUS316L stainless steels. It was demonstrated that LIGA/μ-iMM method actually had a great potential to produce microstructure parts, and it was also confirmed that finer powder was better for their transcription.
  • TAIRA Kensuke; OKUBO Kenji; TANAKA Shigeo; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2004  The Japan Society of Mechanical Engineers
     
    This paper describes the designing techniques for mold in micro metal injection molding, namely μ-MIM. The aim of this study is to investigate the possibility of filling analysis in MIM with commercial-based fluid analytical software for plastic injection molding. The filling length in bar-flow mold of polypropylene was compared the experimental results to analytical ones with variable injection conditions. The filling pattern and inside pressure in the micro dumbbell mold of MIM was also compared in order to investigate the differences between the experimental results and analytical ones.
  • Nishiyabu Kazuaki; Akabane Takahiko; Nonaka Hiroshi
    Symposium on Evaluation and Diagnosis  2003/12
  • マイクロ金属粉末射出成形に適した金型技術の開発  [Not invited]
    西籔和明; 長田俊子; 西上信哉; 柚木明生; 田中茂雄; 松崎 覚; 大久保健児; 平 健輔
    金型技術振興財団 金型に関する研究助成者研究発表会資料  2003/07
  • OSADA Toshiko; NISHIYABU Kazuaki; MATSUZAKI Satoru; TANAKA Shigeo; MIURA Hideshi
    The proceedings of the JSME annual meeting  2003  The Japan Society of Mechanical Engineers
     
    This study describes the micro evaluation methods for investigating the feedstock and component properties and the process conditions for industrial mass production of micro components by Metal Injection Molding (μ-MIM). The effects of feedstock properties such as particle size and powder loading on the sintered properties of micro-dumbbell specimens were investigated under various injection-molding and sintering conditions. Small particle size and high powder loading significantly improved the quality such as density, dimensional accuracy and tensile strength, as well as yield percentage in producing non-defective micro-dumbbell sintered specimens. The surface condition of setting plate in debinding and sintering process influenced on the microstructure of the sintered specimens, i.e. slip-band appeared at only centered narrow segments. Deformation and fracture propagation behaviors were observed with the in-situ SEM tensile test which were useful to comprehend the influences of feedstock quality on the mechanical properties of the μ-MIM products.
  • TAKANO Naoki; ZAKO Masaru; FUJITSU Reiko; NISHIYABU Kazuaki
    The proceedings of the JSME annual meeting  2002  The Japan Society of Mechanical Engineers
     
    To evaluate the moldability and performance of complicated shaped components of textile composites, it is essential to know the large deformation of the textile preform. In this study, a digital image-based strain measurement system is proposed to measure the distribution of large strain in the closed molding based on the theory of continuum mechanics. The Biot's strain is adopted to exclude the misestimation due to the rotational motion during the closed molding. It is calculated with the image capturing and digitization procedures. This report demonstrates the effectiveness of the newly developed method through the application to rib-knitted fabric thermoplastic composites.
  • 成形シミュレーション  [Not invited]
    西籔和明; 仲井朝美; 横山敦士; 濱田泰以
    日本複合材料学会誌  2001
  • Computational and Experimental Anaylysis of Microscopic Large Deformation of Knitted Fabric Composite Material (jointly worked)  [Not invited]
    The 6th Japan International SAMPE Symposium & Exibition  1999
  • Micro Damage Behaviors of Woven Fabric Reinforced Composites with Varied Interfacial Property (jointly worked)  [Not invited]
    Interfacial Phenomena in Composite Materials '99(IPCM '99)  1999
  • Effect of Surface Treatment on the GFRP at the Environmental Creep Conditions(3) (jointly worked)  [Not invited]
    The 7th International Conference on Composite Interfaces(ICCI-(]G0007[))  1998
  • Evaluation of Interfacial Property by Embedded Single Strand Transverse Tensile Test (jointly worked)  [Not invited]
    The 4th International Symposium for Textile Composites(TEXCOMP-4)  1998
  • Fracture Behavior of Concrete Beam Strength with Composite Materials (jointly worked)  [Not invited]
    The 1st Asian-Australasian Conference on Composite Materials(ACCM-1)  1998
  • An Investigation on Micro Damage Behaviors of Woven Fabric Composites with Different Interfacial Property by Experimental and Numerical Analysis (jointly worked)  [Not invited]
    The 4th International Symposium for Textile Composites(TEXCOMP-4)  1998
  • Damage Behaviors of Woven Fabric Composites with Different Interfacial Property (jointly worked)  [Not invited]
    The 1st Asian-Australasian Conference on Composite Materials(ACCM-1)  1998
  • In Situ SEM Observation of Micro Damages under Tensile Load (jointly worked)  [Not invited]
    The 7th International Conference on Composite Interfaces(ICCI-(]G0007[))  1998
  • Effect of Interphase Properties on Initial Damage in Single Fiber Composites under Transverse Tensile Load (jointly worked)  [Not invited]
    The 7th International Conference on Composite Interfaces(ICCI-(]G0007[))  1998
  • Effects of Interphase Properties on Microscopic Damage in Embedded Single Fiber Transverse Tensile Test (jointly worked)  [Not invited]
    The 5th Japan International SAMPE Symposium & Exibition  1997
  • Effect of Interphase Parameters on Stress Distribution in Single Fiber Composites (jointly worked)  [Not invited]
    Interfacial Phenomena in Composite Materials '97(IPCM '97)  1997
  • NISHIYABU Kazuaki; YOKOYAMA Atsushi; HAMADA Hiroyuki
    日本複合材料学会研究発表講演会予稿集  1996/05
  • Assessment of Influence of Interfacial Properties on Stress Transmissibility in Composite by Numerical Approach (jointly worked)  [Not invited]
    The 6th International Conference on Composite Interfaces(ICCI-(]G0006[))  1996
  • Deepdrawing of Knitted Fabric Reinforced Thermoplastic Sheet  [Not invited]
    The 4th Japan International SAMPE Symposium & Exibition  1995

MISC

Industrial Property Rights

Awards & Honors

  • 2008 (社)粉体粉末冶金協会 技術進歩賞
     JPN
  • 2006 (社)日本材料学会 技術賞
     JPN
  • 2006 (社)日本材料学会 関西支部長賞
     JPN
  • 2005 (社)日本機械学会 機械材料・材料加工部門 一般表彰(新技術開発部門)
     JPN
  • 1998 TexComp-4 「Young Researcher Award」
  • 1998 (社)日本材料学会 複合材料部門委員会「奨励賞」
     JPN
  • 2009年度(社)日本機械学会 機械材料・材料加工部門,部門表彰(新技術開発部門)2010.9.6

Research Grants & Projects

  • Japan Society for the Promotion of Science:Grants-in-Aid for Scientific Research
    Date (from‐to) : 2023/04 -2026/03 
    Author : 西籔 和明; 田邉 大貴
  • Japan Society for the Promotion of Science:Grants-in-Aid for Scientific Research
    Date (from‐to) : 2020/04 -2023/03 
    Author : 西籔 和明; 田邉 大貴
     
    本研究は,炭素繊維強化熱可塑性プラスチック(熱可塑性CFRP)の繊維/樹脂界面近傍での融着接合過程の現象解明を目的とし,融着接合部に添加するマイクロ・ナノ粒子の影響を解明した. 具体的には,研究代表者がこれまで独自に取り組んできた金属粉末冶金技術および樹脂射出成形技術を融合したマイクロ・ナノプロセッシングの研究成果を,研究分担者が独自に取り組んできた熱可塑性複合材料の各種融着接合におけるプロセス研究の成果に応用し,分野横断型の学際的な研究を目指した. 研究の結果,熱可塑性複合材料における抵抗融着や誘導融着,超音波融着等の加熱手法の違いや,加熱・加圧・冷却条件などの融着過程に共通する種々の条件,および融着界面におけるカーボンナノチューブ(CNT)などのマイクロ・ナノサイズの粒子や繊維が融着接合過程での繊維/樹脂界面近傍に及ぼす現象や接合強度に及ぼす影響を実験的に解明することができた. 本研究の成果は,熱可塑性樹脂複合材料の融着接合プロセスにおける普遍的な影響因子を明らかにするものであり,熱可塑性CFRP等の先進材料の融着接合プロセスの高度化に貢献できる.これにより,熱可塑性複合材料の用途拡大をより進めることが可能となり,学術的な独創性や工業的有用性は極めて高いと考えられる.また,マイクロ・ナノテクノロジーとCFRPの成形加工技術を融合した先進的な技術分野を開拓し,普遍性の高い研究成果が産業応用につながると考えられる.
  • Japan Society for the Promotion of Science:Grants-in-Aid for Scientific Research
    Date (from‐to) : 2017/04 -2020/03 
    Author : Nishiyabu Kazuaki
     
    This study aims to investigate the fusion bonding interface phenomenon between carbon fiber reinforced thermoplastics (CFRTP) and dissimilar materials such as carbon fiber reinforced thermosetting plastics (CFRP). In order to improve quality of the fusion bonding interface, spread carbon fibers or woven carbon fiber was used as joining layer, and fusion bonding was performed by resistance heating or ultrasonic heating. From the experimental results, it was clarified how to avoid the current leakage to joining target during resistance welding. It was also suggested that the application of micro-sized thermoplastic powder or thermoplastic epoxy polymer to improve the tensile shear strength of the joining part between CFRTP and CFRTP.
  • Japan Society for the Promotion of Science:Grants-in-Aid for Scientific Research
    Date (from‐to) : 2014 -2016 
    Author : NISHIYABU Kazuaki
     
    This study aims to investigate the fabrication method of high functional polymer film with single-digit microstructures by electro-spinning nano-fiber imprinting method which PMMA polymer solution added single nano-particle is electrically span on Si form and melted by heating. The advantages of this novel process author developed are possible high precise transcription of micro-structures by micro-fibril of nano-fiber. From the experimental results, the effect of preparation conditions of spinning solution on the shape transcription of microstructures was investigated. The relationship between viscosity of spinning solution and polymer concentration, and an effect on the diameter of nano-fiber was clarified. It was concluded that the the viscosity of spinning solution was increased, and thus reduced the shape transcription of microstructure was by adding nano-particle.
  • Ministry of Education, Culture, Sports, Science and Technology:Grants-in-Aid for Scientific Research(基盤研究(C))
    Date (from‐to) : 2011 -2013 
    Author : Kazaki NISHIYABU
     
    This study aims to fabricate the micro-structured parts using nano-powder via compaction process by printing. The sacrificial plastic mold (SP-mold) which is derived from melting nanofiber produced by electron spinning (ES) method which provides a simple and versatile method for generating ultra-thin fibers using variety of materials is used. The original form made of silicon has micro-sized structures with line and space patterns, circular hole or column. The material used for printing is the mixture of nano-scale Ni or TiO2 powders and water-soluble binder. It was shown from the results of surface observation that the SP-mold with micro-structures of 1 micron wide and 10 micron high in minimum size could be obtained finely, and also the sound sintered parts were obtained.
  • Ministry of Education, Culture, Sports, Science and Technology:Grants-in-Aid for Scientific Research(基盤研究(C))
    Date (from‐to) : 2008 -2010 
    Author : Kazuaki NISHIYABU
     
    This study aims to develop the manufacturing method of micro-structured parts by the metal powder injection molding (MIM) inserted micro-sacrificial plastic molds which were prepared by nano-imprint lithography (NIL) technique. In this process named NIL/μ-SPiMIM, the feedstock composed of nano-sized copper powder and polyacetal-based binder was adequately prepared and molded into polymethylmethacrylate films with fine line-scan structures, and the molded parts were sintered in a reductive gas atmosphere followed by solvent debinding of the films. The behavior in debinding and sintering was investigated by thermo-gravimetric analysis, carbon and oxygen analysis and SEM observation. The effects of sintering temperature on sintered density and shrinkage, profile accuracy were evaluated systematically. It can be concluded that the manufacturing method named NIL/μ-SPiMIM proposed in this study has great potential to produce precisely 3 dimensional complex metallic parts with fine micro-structures.
  • 炭化珪素繊維強化耐熱複合材料の製造と力学的特性に関する研究
    JAXA:共同研究


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